Thiomorpholine → HCID 59540645, compound
Reaction equation
Br[C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[C:4]([Br:10])[CH:3]=1.[NH:11]1[CH2:16][CH2:15][S:14][CH2:13][CH2:12]1>>[Br:10][C:4]1[CH:3]=[C:2]([N:11]2[CH2:16][CH2:15][S:14][CH2:13][CH2:12]2)[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=1Participants
3
Procedure
This material was prepared starting from 1,3-dibromo-5-methoxy-benzene following general procedures described in these Examples, but using thiomorpholine instead of pyrrolidine.
Workup
- customThis material was prepared
Sources & evidence
- ORD record
- ord-037c24c4bc0a4a2cb20adb04edb2a6f8
- Source dataset
- uspto-grants-2011_08
- Patent number
- US08008298B2
Reaction notes
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