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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1677539Generated: October 29, 2026

Solketal → HCID 59540534, compound

https://huagongshe.com/reaction/1677539

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSolketalHCID 7528—
Reactant2-(Methylthio)ethanolHCID 78925—
ReactantHCID 59541013HCID 59541013—
ProductHCID 59540534HCID 59540534—

Reaction Steps

This material was prepared from 1-[2-[3-(1,1-dioxo-1lambda*6*-thiomorpholin-4-yl)-5-hydroxy-phenyl]-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazin-7-yl]-2,2-dimethyl-propan-1-one via Mitsunobu type alkylation similar to that which was described as above, but using “(2,2-Dimethyl-[1,3]dioxolan-4-yl)-methanol” in place of “2-methylsulfanyl-ethanol”.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08008298B2
Source datasetuspto-grants-2011_08
ORD IDord-32d7ad9f69384a1b9c1c0e29274b04f6
Source noteuspto-grants-2011_08