HuagongsheHuagongshe Chemistry Print Report · For research reference only
n-Heptyl isocyanate → 5-Chloro-2-oxobenzothiazole 3-heptylcarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | n-Heptyl isocyanate | HCID 138341 | — |
| Reactant | 2(3H)-Benzothiazolone, 5-chloro- | HCID 603829 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-Chloro-2-oxobenzothiazole 3-heptylcarboxamide | HCID 131729125 | — |
Reaction Steps
300 mg (1.37 mmol) of 5-chloro-3H-benzothiazol-2-one were reacted in analogy to Example 1 with 174 mg (1.37 mmol) of 1-isocyanatoheptane in dioxane at 80° C. Yield: 100 mg (19%), M+H+: 327.38.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008331B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-5274f2d4d4ba48fa86883c05a0364f45 |
| Source note | uspto-grants-2011_08 |