HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → 4-(3-Chloropropoxy)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 4-Hydroxybenzamide | HCID 65052 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4-(3-Chloropropoxy)benzamide | HCID 14407176 | — |
Reaction Steps
A mixture composed of 0.004 mol of 4-hydroxybenzamide, 0.004 mol of 1-bromo-3-chloropropane and 0.006 mol of caesium carbonate in 10 ml of acetonitrile is heated at reflux for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008337B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-a610f9e58eed4b23a35ff1b7c39edba3 |
| Source note | uspto-grants-2011_08 |