HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R)-3-methyl-1-pyridin-2-ylpiperazine → (3S)-3-methyl-1-pyridin-2-ylpiperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R)-3-methyl-1-pyridin-2-ylpiperazine | HCID 1519493 | — |
| Reactant | 2-Methylpiperazine, (S)- | HCID 2734219 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | (3S)-3-methyl-1-pyridin-2-ylpiperazine | HCID 1519492 | — |
Reaction Steps
The title compound was prepared following the protocol used for the preparation of Intermediate 3, but starting from (S)-2-methyl piperazine (43%). TLC—Chloroform/MeOH (8/2); Rf=0.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008302B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-83b88620e31c4ac0abe12813b211b0c5 |
| Source note | uspto-grants-2011_08 |