HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-bromo-4-(trifluoromethyl)- → HCID 57917051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-bromo-4-(trifluoromethyl)- | HCID 67872 | — |
| Reactant | HCID 11600842 | HCID 11600842 | — |
| Product | HCID 57917051 | HCID 57917051 | — |
Reaction Steps
The title compound was prepared following the procedure of Intermediate 5, but starting from 1-bromo-4-trifluoromethylbenzene. Purification by flash chromatography (CHCl3/MeOH) gave the title compound as a pale yellow solid. M+(ESI): 245.2. HPLC (Condition A), Rt: 2.31 min (HPLC purity: 97.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008302B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-c55760c33b7947aca7e4b3d7b95d0a26 |
| Source note | uspto-grants-2011_08 |