HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-4-tert-butylbenzene → HCID 58487970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-4-tert-butylbenzene | HCID 77595 | — |
| Reactant | HCID 11600842 | HCID 11600842 | — |
| Product | HCID 58487970 | HCID 58487970 | 27% |
Reaction Steps
The title compound was prepared following the procedure of Intermediate 5 but starting from 1-bromo-4-tert-butylbenzene. Purification by chromatography using dichloromethane/methanol (8/2) as eluent afforded The title compound as a liquid (1.5 g, 27%). M+(ESI): 233.3. HPLC (Condition A), Rt: 2.8 min (HPLC purity: 96.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008302B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-f2156c9daab6429f838eeffdc382f9d8 |
| Source note | uspto-grants-2011_08 |