Dimethyl Sulfoxide → 1,1'-Disulfanediylbis(2-chlorobenzene)

Participants

Reaction Steps

Hexamethyldisilazane (4.4 ml) was added to a stirred solution of 2-chlorobenzenethiol (2.0 ml) and DMSO (3.7 ml) in dry acetonitrile at room temperature. After 2 h the white precipitate was filtered and washed (cold acetonitrile) to give the sub-title compound as a white solid (2.27 g).

Provenance & Evidence