Sodium Hydroxide → HCID 86621002, compound

HRID 1677901Notes

Reaction equation

HRID 1677901 reaction equation
[OH-].[Na+:2].[F:3][C:4]([F:21])([F:20])[O:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([OH:19])(=[O:18])=[O:17]>C(O)C>[F:20][C:4]([F:3])([F:21])[O:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([O-:19])(=[O:18])=[O:17].[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 59745701HCID 59745701, compound

Product 1

HCID 86621002HCID 86621002, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

1.15 g (28.8 mmol; 1.3 eq) of NaOH are dissolved in 60 ml of ethanol and added at RT to the sulfonic acid from Example 5c (6.8 g; 22.2 mmol; 1 eq). After refluxing for 1 h, a colourless solid is obtained.

Workup

  1. temperatureAfter refluxing for 1 h
  2. customa colourless solid is obtained

Sources & evidence

ORD record
ord-8101540d600d4b7793ed5a4d44c93832
Source dataset
uspto-grants-2011_08
Patent number
US08008358B2

Reaction notes

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