Sodium Hydroxide → HCID 86621003, compound

HRID 1677902Notes

Reaction equation

HRID 1677902 reaction equation
[Cl:1][CH:2]([CH2:12][S:13]([F:18])([F:17])([F:16])([F:15])[F:14])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][S:8]([OH:11])(=[O:10])=[O:9].[OH-].[Na+:20]>C(O)C>[Cl:1][CH:2]([CH2:12][S:13]([F:18])([F:17])([F:14])([F:15])[F:16])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][S:8]([O-:11])(=[O:10])=[O:9].[Na+:20]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 59745703HCID 59745703, compound

Product 1

HCID 86621003HCID 86621003, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

10g (29.35 mmol; 1 eq) of sulfonic acid from Example 6b are suspended in 130 ml of ethanol, and 1.4 9 (35.22 mmol; 1.2 eq) of sodium hydroxide are added. The reaction mixture is heated under reflux for 1 h. The solid is filtered off at RT.

Workup

  1. temperatureThe reaction mixture is heated
  2. temperatureunder reflux for 1 h
  3. filtrationThe solid is filtered off at RT

Sources & evidence

ORD record
ord-dd9e06f687784bd5840c853c23354438
Source dataset
uspto-grants-2011_08
Patent number
US08008358B2

Reaction notes

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