HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-1H-indole-3-carbaldehyde → HCID 86035888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-1H-indole-3-carbaldehyde | HCID 314791 | — |
| Reactant | 3-Formylphenylboronic acid | HCID 2734356 | — |
| Product | HCID 86035888 | HCID 86035888 | 99% |
Reaction Steps
2-Chloro-1H-indole-3-carboxaldehyde is reacted with 3-formylphenylboronic acid as described in Step 1 of Example 29 to afford 2-chloro-1-(3-formylphenyl)-1H-indole-3-carboxaldehyde (99% yield) as a white solid. ESI/MS 284 (M+H); RT=3.37 min; NMR 10.15 (1H, s); 10.12 (1H, s); 8.23 (3H, m); 7.98 (2H, m); 7.41 (2H, m); 7.18 (1H, d, J=9 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008491B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-fdd3efdb88964209ae84a1ce09d9361a |
| Source note | uspto-grants-2011_08 |