HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyphenylacetyl chloride → N-Cyclohexyl-2-(3-methoxy-phenyl)-2-(2-phenyl-2H-indazol-3-yl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyphenylacetyl chloride | HCID 2733246 | — |
| Reactant | N-Cyclohexyl-2-phenyl-2H-indazol-3-amine | HCID 12318206 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-Cyclohexyl-2-(3-methoxy-phenyl)-2-(2-phenyl-2H-indazol-3-yl)-acetamide | HCID 45110273 | — |
Reaction Steps
In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with 3-methoxyphenyl acetyl chloride ([6834-42-0]) in the presence of Et3N to give the title compound as yellow foam. MS: m/e=440.4 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008505B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-0792a57daabf4eb7b9583501f16226c0 |
| Source note | uspto-grants-2011_08 |