HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2-(4-Chloro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-cyclohexyl-acetic acid → HCID 67131043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2-(4-Chloro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-cyclohexyl-acetic acid | HCID 67131112 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67131043 | HCID 67131043 | — |
Reaction Steps
In analogy to the procedure described in example 29.1, [rac]-[2-(4-chloro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-cyclohexyl-acetic acid (example 5.1) was reduced using borane-tetrahydrofuran complex in THF to give the title compound as off-white solid. MS: m/e=359.2 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008505B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-edb2b0c7e081419c95f670d8c217d4a0 |
| Source note | uspto-grants-2011_08 |