HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine hydrochloride → HCID 178505479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine hydrochloride | HCID 11130 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 45111212 | HCID 45111212 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178505479 | HCID 178505479 | — |
Reaction Steps
In analogy to the procedure described in example 31, [rac]-4-{2-[2-(4-chloro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-2-cyclohexyl-ethoxy}-3-fluoro-benzonitrile (example 37.2) was reacted with sodium azide in the presence of triethylamine hydrochloride in DMF to obtain the title compound as off-white solid. MS: m/e=521.3 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008505B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-b07bf9df4d834605846fb2f4eb10540f |
| Source note | uspto-grants-2011_08 |