HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Trifluoromethylphenoxazine → 2-Trifluoromethyl-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Trifluoromethylphenoxazine | HCID 10467321 | — |
| Reactant | 2-Chloro-1-(1-pyrrolin-2-yl) 2-pyrroline hydrochloride | HCID 20307138 | — |
| Product | 2-Trifluoromethyl-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine | HCID 12799398 | — |
Reaction Steps
Reaction of 2-trifluoromethylphenoxazine with 2-chloro-1-(1-pyrrolin-2-yl)pyrroline hydrochloride according to the procedure of Example 7 affords the free base, 2-TRIFLUOROMETHYL-10-[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]PHENOXAZINE, m.p. 140°-142° C., from n-hexane. Conversion of the free base affords 2-TRIFLUOROMETHYL-10[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]PHENOXAZINE HYDROCHLORIDE HYDRATE, m.p. 222.5°-229° C. (dec.) (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077959 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-11b93ac7a6384513bf620b6694f0e76f |
| Source note | uspto-grants-1978_03 |