Sodium borohydride → HCID 20364510, compound

HRID 1678883Notes

Reaction equation

[OH:1][C:2]1([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[CH2:7][CH2:6][N:5]([CH2:8][CH2:9][CH2:10][CH2:11][N:12]2[C:21](=[O:22])[C:20]3[CH:23]=[CH:24][CH:25]=[C:18]4[C:19]=3[C:14](=[CH:15][CH:16]=[CH:17]4)[C:13]2=[O:26])[CH2:4][CH2:3]1.[BH4-].[Na+]>>[OH:1][C:2]1([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[CH2:3][CH2:4][N:5]([CH2:8][CH2:9][CH2:10][CH2:11][N:12]2[CH:21]([OH:22])[C:20]3[CH:23]=[CH:24][CH:25]=[C:18]4[C:19]=3[C:14](=[CH:15][CH:16]=[CH:17]4)[C:13]2=[O:26])[CH2:6][CH2:7]1

Participants

Reactant 2

HCID 4311764Sodium borohydride

HCID 20364462HCID 20364462, compound

Product 1

HCID 20364510HCID 20364510, compound

Procedure

The product from part (a) is reacted with sodium borohydride as taught in either example 1 or 38 to yield the titled compound.

Sources & evidence

ORD record: ord-41bd87811a454b599ae9745ee4492a43
Source dataset: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04077958

Reaction notes

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