HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycerol → 2-(2-Ethoxyphenyl)-5-hydroxy-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Benzaldehyde, 2-ethoxy- | HCID 11950 | — |
| Product | 2-(2-Ethoxyphenyl)-5-hydroxy-1,3-dioxane | HCID 20364927 | — |
Reaction Steps
Using the method of Example 5e, 30 g 2-ethoxybenzaldehyde was reacted with 18.4 g glycerol to form 2-(2-ethoxyphenyl)-5-hydroxy-1,3-dioxane, crude b.p. 140°-148° C/10-5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-963cef6349be4dc2baaa407fcb2b301d |
| Source note | uspto-grants-1978_03 |