HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 5-Benzyloxy-2,2-dimethyl-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-Benzyloxy-2,2-dimethyl-1,3-dioxane | HCID 20364889 | — |
Reaction Steps
Using the procedure of Example 51, 2-benzyloxy-1,3-propanediol and acetone were reacted, using benzene as solvent, to give, after distillation using a short path column, 5-benzyloxy-2,2-dimethyl-1,3-dioxane. The nmr spectrum was consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-80f56de90df74adaade2cd08e85c9ee3 |
| Source note | uspto-grants-1978_03 |