Chloride → n-Octylsuccinyl dichloride

HRID 1679154노트

반응식

HRID 1679154 반응식
[CH2:1]([CH:9]1[CH2:14][C:13](=[O:15])O[C:10]1=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].P(Cl)(Cl)(Cl)(Cl)[Cl:17].[Cl-:22]>>[CH2:1]([CH:9]([CH2:14][C:13]([Cl:17])=[O:15])[C:10]([Cl:22])=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 3

HCID 312ChlorideHCID 24819Phosphorus pentachlorideHCID 778692,5-Furandione, dihydro-3-octyl-

생성물 1

HCID 23345517n-Octylsuccinyl dichloride수율 79.2%

실험 절차

n-Octylsuccinyl dichloride was prepared by reacting n-octylsuccinic anhydride with PCl5 at 105°-110° C for about four hours. After working the product up 101.3 g of liquid was obtained which had a purity of 84.3% according to chloride content. The corrected yield was 79.2%.

후처리

  1. customat 105°-110° C
  2. customfor about four hours
  3. customwas obtained which

출처 및 근거

ORD 기록
ord-87e2ce8cd2ff404580f820793c426d82
출처 데이터셋
uspto-grants-1978_03
특허 번호
US04079074

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