Ammonia → HCID 20364090, compound

HRID 1679173Notes

Reaction equation

HRID 1679173 reaction equation
[N:1]1([CH:6]([CH2:12][CH2:13][CH2:14][CH3:15])[C:7](OCC)=[O:8])[CH:5]=[N:4][CH:3]=[N:2]1.[NH3:16]>>[N:1]1([CH:6]([CH2:12][CH2:13][CH2:14][CH3:15])[C:7]([NH2:16])=[O:8])[CH:5]=[N:4][CH:3]=[N:2]1

Participants

3

Reactant 2

HCID 222AmmoniaHCID 20364095HCID 20364095, compound

Product 1

HCID 20364090HCID 20364090, compound

Procedure

Ethyl α-1,2,4-triazol-1-ylcaproate (3.0 g) was added to liquid ammonia (0.880, 15 ml) and the mixture was shaken well for a few minutes and then left overnight at room temperature. The white solid was filtered and washed with water to give, after recrystallisation from water, the title compound.

Workup

  1. filtrationThe white solid was filtered
  2. washwashed with water
  3. customto give
  4. customafter recrystallisation from water

Sources & evidence

ORD record
ord-f30040ddb939454fb7ae8d18d2d10fbf
Source dataset
uspto-grants-1978_03
Patent number
US04079143

Reaction notes

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