Glycol monoethyl ether → HCID 20362179, compound

HRID 1679250Notes

Reaction equation

HRID 1679250 reaction equation
[C:1]([C:9]1[CH:17]=[CH:16][C:12]([C:13](Cl)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:18]([O:20][CH2:21][CH2:22][OH:23])[CH3:19]>>[CH2:18]([O:20][CH2:21][CH2:22][O:23][C:13](=[O:14])[C:12]1[CH:11]=[CH:10][C:9]([C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[CH:17][CH:16]=1)[CH3:19]

Participants

3

Reactant 2

HCID 8076Glycol monoethyl etherHCID 129121414-Benzoylbenzoyl chloride

Product 1

HCID 20362179HCID 20362179, compound

Procedure

(2-Ethoxyethyl)-p-benzoylbenzoate was prepared from para-benzoyl benzoic acid chloride and 2-ethoxyethanol. The structure of the product was confirmed by the presence of carbonyl bands in the infrared spectrum at 1670 and 1730 cm-1. When added at 4% by weight loading to the solution described in Example 1, a cure rate of 15 ft./min./lamp was obtained. A sample in the same test solution was stable after three months storage following the procedure described in Example 5.

Workup

  1. additionWhen added at 4% by weight loading to the solution
  2. customa cure rate of 15 ft./min./lamp was obtained
  3. waitA sample in the same test solution was stable after three months

Sources & evidence

ORD record
ord-fec985d4b8af417fb63090d0c2c1a83b
Source dataset
uspto-grants-1978_03
Patent number
US04080275

Reaction notes

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