2-(Dimethylamino)ethanol → Benzoic acid, 4-benzoyl-, 2-(dimethylamino)ethyl ester

HRID 1679251Notes

Reaction equation

HRID 1679251 reaction equation
[C:1]([C:9]1[CH:17]=[CH:16][C:12]([C:13](Cl)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21][OH:22]>>[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21][O:22][C:13](=[O:14])[C:12]1[CH:11]=[CH:10][C:9]([C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 79022-(Dimethylamino)ethanolHCID 129121414-Benzoylbenzoyl chloride

Product 1

HCID 679954Benzoic acid, 4-benzoyl-, 2-(dimethylamino)ethyl ester

Procedure

(2-Dimethylaminoethyl)-p-benzoylbenzoate was prepared from para-benzoylbenzoic acid chloride and 2-dimethylaminoethanol. The structure of the product was confirmed by the presence of carbonyl absorption bands in the infrared spectrum at 1670 and 1725 cm-1. When added at 4% by weight loading to the test solution described in Example 3, a cure rate of 40 ft./min./lamp was observed.

Workup

  1. customThe structure of the product was confirmed by the presence of carbonyl absorption bands in the infrared spectrum at 1670 and 1725 cm-1
  2. additionWhen added at 4% by weight loading to the test solution

Sources & evidence

ORD record
ord-9c46615e2a714c3e84bc898ef6e48f74
Source dataset
uspto-grants-1978_03
Patent number
US04080275

Reaction notes

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