HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetic Acid → HCID 12661864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetic Acid | HCID 300 | — |
| Reactant | HCID 12661846 | HCID 12661846 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 12661864 | HCID 12661864 | 92% |
Reaction Steps
To a solution of 73.3 g (0.744 mol) chloroacetic acid in 700 ml 12N HCl was added 28.6 g (0.122 mol) of 5-m-tolyloxy-2-thiouracil. The slurry was heated at reflux for 35 hours and filtered while still hot. The resulting white solid was washed well with H2O and dried to give 24.5 g of 5-m-tolyloxyuracil (m.p. 291°-295°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080454 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-369d43da719b4a07bad3244516be0b82 |
| Source note | uspto-grants-1978_03 |