HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Bis(methylthio)-2-nitroethylene → HCID 178526914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | 2-(3-Chloropyrid-2-ylmethylthio)ethylamine | HCID 12951532 | — |
| Reactant | HCID 178503827 | HCID 178503827 | — |
| Reactant | HCID 178511474 | HCID 178511474 | — |
| Product | HCID 178526914 | HCID 178526914 | — |
Reaction Steps
4-[2-(2-Aminoethylthio)ethyl]imidazole (from the dihydrobromide (4.0 g) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) by the procedure of Example 8(i) and the resultant 1-nitro-2-methylthio-2-[2-(2-(4-imidazolyl)ethylthio)ethylamino]ethylene is treated with 2-[(2-aminoethyl)thiomethyl]-3chloropyridine by the procedure of Example 1(a)(ii) to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080459 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-510d8d72cc25447999e3c147162518ed |
| Source note | uspto-grants-1978_03 |