HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13860722, compound → 4-(Benzenesulfonyl)benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13860722 | HCID 13860722 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(Benzenesulfonyl)benzene-1,2-diamine | HCID 13860723 | — |
Reaction Steps
1.9 g. of 2-amino-1-nitro-4-phenylsulfonylbenzene is treated in methanol with hydrogen at 4 atmospheres in the presence of Raney nickel catalyst for 2 hours. The catalyst if filtered off and the filtrate stripped under vacuum. Recrystallization of the residue gives 1,2-diamino-4-phenylsulfonylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080461 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-06cfadf0517d4487af378fe1981ae19e |
| Source note | uspto-grants-1978_03 |