HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monobenzone → ((p-(Benzyloxy)phenoxy)methyl)oxirane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monobenzone | HCID 7638 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Product | ((p-(Benzyloxy)phenoxy)methyl)oxirane | HCID 119882 | — |
Reaction Steps
25 g of p-benzyloxyphenol, 165 ml of epichlorohydrin, and 34.5 g of potassium carbonate were refluxed while stirring for 4 hours. The mixture was cooled down to room temperature and filtered, whereupon it was evaporated to dryness. The product was recrystallized from the smallest possible amount of diisopropyl ether. M.p. 68° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080471 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-cd07c1cec65643e3bbff8bdde7248dba |
| Source note | uspto-grants-1978_03 |