Furfurylamine → HCID 178478539, compound

Participants

Reaction Conditions

Reaction Steps

A mixture consisting fo 6.0 gm (0.0202 mol) of 2-methylmercapto-4-(2',6'-dichloro-phenyl)-2-imidazoline hydrochloride and 2.8 gm (0.029 mol) of furfurylamine was heated for 30 minutes at 140° C. The resulting dark-brown mass was dissolved in ethanol and then crystallized by addition of acetone and ether; for further purification, the crystallizate was again dissolved in ethanol and acetone, reprecipitated by addition of ether, and recrystallized from water, yielding 2.5 gm (35.7% of theory) of the yellow crystalline compound of the formula ##STR12## which had a melting point of 191° C.

Provenance & Evidence