1,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl- → HCID 70575974, compound

HRID 1679495Notes

Reaction equation

HRID 1679495 reaction equation
[Cl:1]N1C(=O)NC(=O)N(Cl)C1=O.[Na].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][N:15]1[CH3:23]>CO>[Cl-:1].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][NH+:15]1[CH3:23]

Participants

4

Reactant 2

HCID 1816881,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl-HCID 866576592893-78-9

Product 1

HCID 70575974HCID 70575974, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

17.8 g (0.1 mol) of sodium dichlorocyanuric acid are added to 15.7 g (0.1 mol) of 2,4-dioxo-hexahydro-1,3,5-trimethyl-s-triazine in 50 ml of methanol and the mixture is stirred. The cyanuric acid which has precipitated is then filtered off and the filtrate is evaporated. The residue which remains on evaporation is digested with water. After renewed filtration to remove residual cyanuric acid, an aqueous solution of the same compound as in Example g is obtained.

Workup

  1. customThe cyanuric acid which has precipitated
  2. filtrationis then filtered off
  3. customthe filtrate is evaporated
  4. customThe residue which remains on evaporation
  5. filtrationfiltration
  6. customto remove residual cyanuric acid
  7. customan aqueous solution of the same compound as in Example g is obtained

Sources & evidence

ORD record
ord-3769b7e41fcb49179062e8fdcf5f8766
Source dataset
uspto-grants-1978_03
Patent number
US04080502

Reaction notes

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