HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → HCID 136388399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | 2-Naphthalenol, 1-(3-pyridinylazo)- | HCID 73745 | — |
| Product | HCID 136388399 | HCID 136388399 | — |
Reaction Steps
A mixture of 50.3 pounds of sodium chloride and 3.7 pounds (6.75 moles) of 1-(3-pyridylazo)-2-naphthol is blended in a Patterson-Kelly liquid-solid blender and 2.89 pounds (7.05 moles) of methyl p-toluenesulfonate added thereto over a period of about 45 minutes. The temperature of the reaction is maintained at about 40°-50° C for an additional period of about one hour. The product is of acceptable purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04081436 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-dff637b14b4e4493bfd3fc9579766325 |
| Source note | uspto-grants-1978_03 |