Methyl Isocyanate → HCID 53832727, compound

HRID 1680120Notes

Reaction equation

HRID 1680120 reaction equation
[CH3:1][CH:2]([NH2:17])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH3:18][N:19]=[C:20]=[O:21]>C(Cl)Cl>[CH3:1][CH:2]([NH:17][C:20]([NH:19][CH3:18])=[O:21])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 12228Methyl IsocyanateHCID 18179237Hexadecan-2-amine

Product 1

HCID 53832727HCID 53832727, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent2×

Procedure

38.6 g (0.135 mole) beta-hexadecylamine in 60 ml methylene chloride was reacted with 9.6 ml methyl isocyanate in 15 ml methylene chloride in accordance with the procedure in Example 4, yielding a white solid reaction product.

Workup

  1. customyielding
  2. customa white solid reaction product

Sources & evidence

ORD record
ord-14ca957df78a4a75ab3480e01e501c18
Source dataset
uspto-grants-1981_06
Patent number
US04272413

Reaction notes

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