Hydrogen Bromide → HCID 54251945, compound

Participants

Reaction Steps

2.84 g of the alcohol III prepared as described in Example 1 were dissolved in 50 ml of ether and an equimolar amount of a solution of HBr in ether was added dropwise at -70° C., whilst stirring. The reaction mixture was then kept for 15 minutes at from -60° to -70° C. and thereafter for 15 minutes at -15° C. 30 ml of water were then added and the organic phase was separated off, washed neutral, dried and concentrated. 3.2 g of a residue (crude yield 93.5%) were left; the structure of the material was determined by IR, NMR and UV spectroscopy.

Provenance & Evidence