Chloroacetyl chloride → HCID 54185631, compound
Reaction equation
[CH3:1][NH:2][C:3]12[CH2:12][CH:8]([CH2:9][CH2:10][CH2:11]1)[CH:7]1[CH2:13][CH:4]2[CH2:5][CH2:6]1.[Cl:14][CH2:15][C:16](Cl)=[O:17]>>[CH3:1][N:2]([C:3]12[CH2:12][CH:8]([CH2:9][CH2:10][CH2:11]1)[CH:7]1[CH2:13][CH:4]2[CH2:5][CH2:6]1)[C:16](=[O:17])[CH2:15][Cl:14]Participants
3
Procedure
Under the same conditions as described in section (A) of Example 4, 1-methylaminotricyclo[4.3.1.12,5 ]undecane was reacted with 2-chloroacetyl chloride to obtain N-methyl-N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-chloroacetamide in a yield of 85%.
Sources & evidence
- ORD record
- ord-e9dcfd266a5849be9deb5e8018716838
- Source dataset
- uspto-grants-1981_06
- Patent number
- US04272536
Reaction notes
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