Phthalimide potassium salt → HCID 53852519, compound

HRID 1680184Notes

Reaction equation

HRID 1680184 reaction equation
[CH3:1][N:2]([C:7]12[CH2:16][CH:12]([CH2:13][CH2:14][CH2:15]1)[CH:11]1[CH2:17][CH:8]2[CH2:9][CH2:10]1)[C:3](=[O:6])[CH2:4]Cl.[C:18]1(=[O:28])[NH:22][C:21](=[O:23])[C:20]2=[CH:24][CH:25]=[CH:26][CH:27]=[C:19]12.[K]>>[CH3:1][N:2]([C:7]12[CH2:16][CH:12]([CH2:13][CH2:14][CH2:15]1)[CH:11]1[CH2:17][CH:8]2[CH2:9][CH2:10]1)[C:3](=[O:6])[CH2:4][N:22]1[C:21](=[O:23])[C:20]2=[CH:24][CH:25]=[CH:26][CH:27]=[C:19]2[C:18]1=[O:28]

Participants

3

Reactant 2

HCID 24194345Phthalimide potassium saltHCID 54185631HCID 54185631, compound

Product 1

HCID 53852519HCID 53852519, compoundYield 83%

Procedure

Under the same reaction conditions as described in section (A) of Example 7, N-methyl-N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-chloroacetamide was reacted with potassium phthalimide to obtain N-methyl-N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-phthalimidoacetamide in a yield of 83%.

Workup

  1. customUnder the same reaction conditions

Sources & evidence

ORD record
ord-71fb1da0a7694452bc1d5e08e8abf22a
Source dataset
uspto-grants-1981_06
Patent number
US04272536

Reaction notes

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