Ethanol → HCID 54224739, compound

HRID 1680266Notes

Reaction equation

HRID 1680266 reaction equation
[C:1]([C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][C:17]=1[OH:18])[CH:14]([C:19]([OH:21])=[O:20])[CH2:13][CH2:12]2)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.S(=O)(=O)(O)O.[CH2:27](O)[CH3:28]>>[CH2:27]([O:20][C:19]([CH:14]1[C:15]2[C:11](=[CH:10][C:9]([C:1](=[O:8])[C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)=[C:17]([OH:18])[CH:16]=2)[CH2:12][CH2:13]1)=[O:21])[CH3:28]

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 688795-Benzoyl-6-hydroxy-2,3-dihydro-1H-indene-1-carboxylic acid

Product 1

HCID 54224739HCID 54224739, compound

Procedure

Analogously to Example 3, 12 g of 5-benzoyl-6-hydroxyindane-1-carboxylic acid and ethanol containing sulphuric acid give 5-benzoyl-6-hydroxy-indane-1-carboxylic acid ethyl ester in the form of yellow platelets of melting point 83°-4° C.

Sources & evidence

ORD record
ord-9b53fbc8a8f3481caacb2f20a52e7d51
Source dataset
uspto-grants-1981_06
Patent number
US04272547

Reaction notes

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