HCID 53783109, compound → HCID 23457887, compound

HRID 1680268Notes

Reaction equation

HRID 1680268 reaction equation
C[O:2][C:3]([CH:5]1[C:13]2[C:8](=[CH:9][C:10]([C:15]([C:17]3[CH:22]=[CH:21][C:20]([CH3:23])=[CH:19][CH:18]=3)=[O:16])=[C:11]([OH:14])[CH:12]=2)[CH2:7][CH2:6]1)=[O:4]>CCOCC>[C:20]1([CH3:23])[CH:21]=[CH:22][C:17]([C:15]([C:10]2[CH:9]=[C:8]3[C:13](=[CH:12][C:11]=2[OH:14])[CH:5]([C:3]([OH:4])=[O:2])[CH2:6][CH2:7]3)=[O:16])=[CH:18][CH:19]=1

Participants

3

Reactant 1

HCID 53783109HCID 53783109, compound

Product 1

HCID 23457887HCID 23457887, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Analogously to the method described in Example 2, 8.5 g of 5-(p-toluoyl)-6-hydroxy-indane-1-carboxylic acid methyl ester give 5-(p-toluoyl)-6-hydroxy-indane-1-carboxylic acid in the form of yellow crystals of melting point 186°-8° C. (from ether).

Sources & evidence

ORD record
ord-8c138152d1d64b64b7b0a754cb016a3f
Source dataset
uspto-grants-1981_06
Patent number
US04272547

Reaction notes

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