HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 23457770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Acetone Cyanohydrin | HCID 6406 | — |
| Reactant | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 23457770 | HCID 23457770 | — |
Reaction Steps
A stirred solution of 20 g. (48.0 m moles) 4-(hexadecylamino)benzoyl chloride hydrochloride in 500 ml. acetone and 50 ml. pyridine is cooled in an ice-water bath, and to this in portions is added 4.3 g. (51 m moles) acetone cyanohydrin. The solution is warmed to room temperature and stirred for an additional two hours. The solvents are evaporated to a yellow gum, which crystallizes to off-white crystals from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272546 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-c7f1a456ec914d25a07668499f6c0d08 |
| Source note | uspto-grants-1981_06 |