HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 1-Carbamoylethyl 4-(hexadecylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1-Cyanoethyl 4-(hexadecylamino)benzoate | HCID 23457872 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Carbamoylethyl 4-(hexadecylamino)benzoate | HCID 23457803 | — |
Reaction Steps
A mixture of 5 g. (12.1 m moles) 1-cyanoethyl 4-(hexadecylamino)benzoate in 100 ml. 75% sulfuric acid is heated at 50° C. for 20 hours. The cooled solution is diluted with water, filtered, and the residue is dried to yield the amide as a white amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272546 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-ce66d713bf944ff4a8c2fcd094904fb5 |
| Source note | uspto-grants-1981_06 |