HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54439614, compound → HCID 23457838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54439614 | HCID 54439614 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23457838 | HCID 23457838 | — |
Reaction Steps
A solution of 4 g. (8.7 m moles) 2-(ethoxycarbonyl)vinyl 4-(hexadecylamino)benzoate and 400 mg. 10% Pd(C) in 100 ml. tetrahydrofuran is hydrogenated at 50 psi until hydrogen uptake stops. The catalyst is filtered, the solution is evaporated, and the residue is crystallized from acetonitrile to yield 2-(ethoxycarbonyl)ethyl 4-(hexadecylamino)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272546 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-d4bded2188df472bb7c1cdce0a3e9f59 |
| Source note | uspto-grants-1981_06 |