Sodium Hydroxide → Sodium 4-(14-methylpentadecylamino)benzoate

HRID 1680299Notes

Reaction equation

HRID 1680299 reaction equation
[CH3:1][CH:2]([CH3:26])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH:16][C:17]1[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1.[OH-].[Na+:28]>C(O)C>[CH3:1][CH:2]([CH3:26])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH:16][C:17]1[CH:18]=[CH:19][C:20]([C:21]([O-:23])=[O:22])=[CH:24][CH:25]=1.[Na+:28]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 204373644-(14-Methylpentadecyl)aminobenzoic acid

Product 1

HCID 23686414Sodium 4-(14-methylpentadecylamino)benzoate

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of 10 g. (27.7 m moles) 4-(14-methylpentadecylamino)benzoic acid in 300 ml. hot ethanol is added 6.0 ml. (1.1 eq) 5 N sodium hydroxide. As the solution cools, the title compound crystallizes as a white mass. This is collected and dried in vacuo.

Workup

  1. customAs the solution cools, the title compound crystallizes as a white mass
  2. customThis is collected
  3. customdried in vacuo

Sources & evidence

ORD record
ord-d2a216034f39443792064fcb13ca33f8
Source dataset
uspto-grants-1981_06
Patent number
US04272546

Reaction notes

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