HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 814775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Aminopyridine | HCID 1727 | — |
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Product | HCID 814775 | HCID 814775 | — |
| Product | HCID 54498242 | HCID 54498242 | — |
Reaction Steps
β-(phenyl)-N-(4-pyridyl)propionamide is prepared by reacting 4-aminopyridine with β-(phenyl)propionyl chloride in pyridine at room temperature. The amide is reduced to give the title compound by treating a solution of the amide in dry tetrahydrofuran stirred and cooled to 0° C. with diborane in a stream of nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272628 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-710fd5ba1ac742f2a0b9c5ad81c5410e |
| Source note | uspto-grants-1981_06 |