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HRID1680612

反应详情

EQUATION

反应方程式

HRID 1680612 的结构方程式

REACTANTS

反应物

2
结构：CNN
HCID6061

Methylhydrazine

CH6N2

结构：CSC1=NCCN1.I
HCID12221228

2-(Methylsulfanyl)-4,5-dihydro-1H-imidazole--hydrogen iodide (1/1)

C4H9IN2S

PRODUCTS

生成物

1
结构：CN(N)C1=NCCN1.I
HCID20536309

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

CONDITIONS

反应条件

温度
-10 °C

PROCEDURE

实验过程

A solution of 48.8 g. of 2-methylthio-2-imidazoline hydroiodide and 10.0 g. of methylhydrazine in 200 ml. of ethanol is heated at reflux for several hours, clarified and then cooled at -10° C. The precipitate is collected, washed with diethyl ether and dried, giving 2-(1-methylhydrazino)imidazoline hydroiodide.

WORKUP

后处理

  1. temperatureat reflux for several hours
  2. customThe precipitate is collected
  3. washwashed with diethyl ether
  4. customdried