HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylaniline → HCID 13071317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | p-Toluenesulfonic acid 1-butyn-3-yl ester | HCID 561098 | — |
| Product | HCID 13071317 | HCID 13071317 | — |
Reaction Steps
22.4 g of 1-butyn-3-ol tosylate in 26 g of 2,6-dimethylaniline are stirred at 110° C. for 3 hours. The mixture is then poured into ice-water, extracted with ethyl acetate, dried over sodium sulfate and filtered. The solvent is distilled off to yield N-(1-methyl-2-propynyl)-2,6-xylidine; b.p. 68°-72° C./0.05 Torr; m.p. 32°-33° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04275079 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-aa4b3f6f0e8c4f6488cadf8c7bfa4c08 |
| Source note | uspto-grants-1981_06 |