HRID1680656

反应详情

EQUATION

反应方程式

HRID 1680656 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 4.7 g (0.020 mol) of 4-(α-naphthoxy)-aniline in 100 ml of absolute toluene were added 3.65 g (0.020 mol) of o-chlorobenzoyl isocyanate. The reaction solution thus obtained was stirred at room temperature for 15 hours. During this time the product crystallized out. It was removed by suction filtration, washed with toluene, and dried.

WORKUP

后处理

  1. customThe reaction solution thus obtained
  2. customDuring this time the product crystallized out
  3. customIt was removed by suction filtration
  4. washwashed with toluene
  5. customdried