4-(naphthalen-1-yloxy)aniline → HCID 23455392, compound

HRID 1680656Notes

Reaction equation

HRID 1680656 reaction equation
[C:1]1([O:11][C:12]2[CH:18]=[CH:17][C:15]([NH2:16])=[CH:14][CH:13]=2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[Cl:19][C:20]1[CH:30]=[CH:29][CH:28]=[CH:27][C:21]=1[C:22]([N:24]=[C:25]=[O:26])=[O:23]>C1(C)C=CC=CC=1>[C:1]1([O:11][C:12]2[CH:18]=[CH:17][C:15]([NH:16][C:25]([NH:24][C:22](=[O:23])[C:21]3[CH:27]=[CH:28][CH:29]=[CH:30][C:20]=3[Cl:19])=[O:26])=[CH:14][CH:13]=2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 8195834-(naphthalen-1-yloxy)anilineHCID 99423112-Chlorobenzoyl isocyanate

Product 1

HCID 23455392HCID 23455392, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of 4.7 g (0.020 mol) of 4-(α-naphthoxy)-aniline in 100 ml of absolute toluene were added 3.65 g (0.020 mol) of o-chlorobenzoyl isocyanate. The reaction solution thus obtained was stirred at room temperature for 15 hours. During this time the product crystallized out. It was removed by suction filtration, washed with toluene, and dried.

Workup

  1. customThe reaction solution thus obtained
  2. customDuring this time the product crystallized out
  3. customIt was removed by suction filtration
  4. washwashed with toluene
  5. customdried

Sources & evidence

ORD record
ord-319b6bae1dfd4a0b9805297a3f7aa1be
Source dataset
uspto-grants-1981_06
Patent number
US04275077

Reaction notes

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