HRID1680656
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 4.7 g (0.020 mol) of 4-(α-naphthoxy)-aniline in 100 ml of absolute toluene were added 3.65 g (0.020 mol) of o-chlorobenzoyl isocyanate. The reaction solution thus obtained was stirred at room temperature for 15 hours. During this time the product crystallized out. It was removed by suction filtration, washed with toluene, and dried.
WORKUP
后处理
- customThe reaction solution thus obtained
- customDuring this time the product crystallized out
- customIt was removed by suction filtration
- washwashed with toluene
- customdried