HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl bromide | HCID 54508681 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl iodide | HCID 53794750 | — |
Reaction Steps
3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl iodide [VI; Ar is 3,4-methylenedioxyphenyl, R is CH3 ] was prepared from 19.0 g. of 3-methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl bromide (Preparation C3) and 10.5 g. of sodium iodide in 125 ml. of acetone, to give 21 g. of product as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04275201 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-73c10c39580e4ca2bbfff1f161b10ae3 |
| Source note | uspto-grants-1981_06 |