Hydrochloric Acid → HCID 88761779, compound

Participants

Reaction Steps

A solution of 1.76 g; 4.34 mmol of compound VIII in 48 ml of anhydrous methylene dichloride was saturated at 0° C. with anhydrous hydrogen chloride. The resulting precipitate of p-nitrobenzoic acid was filtered off under anhydrous conditions and the filtrate was evaporated to give a residue of 1.2 g (yield 100%) of 4-O-methyl-2,3,6-trideoxy-3-trifluoroacetamido-L-ribohexopyranosyl chloride (III).

Provenance & Evidence