HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1680887Generated: November 1, 2026
Dimethyl Sulfoxide → alpha-(alpha,alpha-Dimethyl-2,3,4-trimethoxyphenethylimino)-2-methoxyacetophenone
https://huagongshe.com/reaction/1680887
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | 2-Methyl-1-(2,3,4-trimethoxyphenyl)propan-2-amine | HCID 13020597 | — |
| Reactant | 2-Methoxyphenylglyoxal hydrate | HCID 20434110 | — |
| Product | alpha-(alpha,alpha-Dimethyl-2,3,4-trimethoxyphenethylimino)-2-methoxyacetophenone | HCID 23454833 | — |
Reaction Steps
A solution of 133 mg of α,α-dimethyl-2,3,4-trimethoxyphenethylamine in 1.5 ml of dimethylsulfoxide is added to 111 mg of 2-methoxyphenylglyoxal hydrate, and the mixture is stirred at 20° C. for one hour, whereby a solution of α-(α,α-dimethyl-2,3,4-trimethoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04276304 |
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| Source dataset | uspto-grants-1981_06 |
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| ORD ID | ord-d9c89c4dfa1c4c26bef4105832ba69f9 |
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| Source note | uspto-grants-1981_06 |
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