Dimethyl Sulfoxide → HCID 86737826, compound

HRID 1680889Notes

Reaction equation

HRID 1680889 reaction equation
O.CO[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]([CH:12]=[O:13])=[O:11].[CH3:14][C:15]([NH2:27])([CH3:26])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]2[O:23][CH2:24][O:25][C:19]=2[CH:18]=1.[CH3:28]S(C)=O>>[CH3:26][C:15]([N:27]=[C:12]([O:13][CH3:28])[C:10]([C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:11])([CH3:14])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]2[O:23][CH2:24][O:25][C:19]=2[CH:18]=1

Participants

4

Reactant 3

HCID 679Dimethyl Sulfoxide2×HCID 130205981-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amineHCID 204341102-Methoxyphenylglyoxal hydrate

Product 1

HCID 86737826HCID 86737826, compound

Procedure

A mixture of 590 mg of 2-methoxyphenylglyoxal hydrate, 500 mg of α,α-dimethyl-3,4-methylenedioxyphenethylamine and 1.5 ml of dimethylsulfoxide is stirred at room temperature for 45 minutes, whereby a solution of α-(α,α-dimethyl-3,4-methylenedioxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.

Sources & evidence

ORD record
ord-b9cc545c0a69492ebf048695cb11574d
Source dataset
uspto-grants-1981_06
Patent number
US04276304

Reaction notes

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