HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldiimidazole → HCID 20454059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Reactant | Acetic acid, 2-(4-aminophenyl)hydrazide | HCID 81068 | — |
| Reactant | HCID 23454956 | HCID 23454956 | — |
| Product | HCID 20454059 | HCID 20454059 | — |
Reaction Steps
4-(2-Acetylhydrazino)phenyl isothiocyanate was prepared as described for NA-11 in Example 4 with 1-acetyl-2-(4-aminophenyl)hydrazine (1.23 g, 0.0075 mole) and 1,1'-thiocarbonyldiimidazole (1.35 g, 0.0075 mole). Yield 1.20 g (77 percent), m.p. 172°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04276364 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-a5acd6a6acba45bf8b94e6f4a43edd0d |
| Source note | uspto-grants-1981_06 |