Morpholine → HCID 23454965, compound

HRID 1680900Notes

Reaction equation

HRID 1680900 reaction equation
[NH:1]1[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[CH:7]([NH:9][NH:10][C:11]1[CH:16]=[CH:15][C:14]([N:17]=[C:18]=[S:19])=[CH:13][CH:12]=1)=[O:8].C(NNC1C=CC(NC(N(CC2C=CC=CC=2)CC2C=CC=CC=2)=S)=CC=1)=O>>[CH:7]([NH:9][NH:10][C:11]1[CH:16]=[CH:15][C:14]([NH:17][C:18]([N:1]2[CH2:6][CH2:5][O:4][CH2:3][CH2:2]2)=[S:19])=[CH:13][CH:12]=1)=[O:8]

Participants

4

Reactant 3

HCID 8083MorpholineHCID 20283022N'-(4-Isothiocyanatophenyl)formohydrazideHCID 23454956HCID 23454956, compound

Product 1

HCID 23454965HCID 23454965, compound

Procedure

Morpholine (0.087 g, 0.001 mole) and 4-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.22 g (79 percent), m.p. 204°-206° C.

Sources & evidence

ORD record
ord-c9a76e1b793f4cc995ca001c41520b26
Source dataset
uspto-grants-1981_06
Patent number
US04276364

Reaction notes

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