HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyldichlorosilane → Dichloro(methyl)(2-phenylpropyl)silane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyldichlorosilane | HCID 6376 | — |
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Reactant | HCID 22023791 | HCID 22023791 | — |
| Product | Dichloro(methyl)(2-phenylpropyl)silane | HCID 114552 | — |
Reaction Steps
The process described in Example 2 is repeated, except that 1.3 liters of methyldichlorosilane, 1.7 liters of 1-methylstyrene and 5 ml of the catalytic solution are substituted for the trichlorosilane, allyl chloride and catalytic solution and the process is carried out at a temperature of 140° C. instead of 120° C. About 97.9 mol percent of the methyldichlorosilane used is converted and 12.8 moles per hour of 2-phenyl-2-methylethyl (methyl) dichlorosilane are obtained having a purity of 97.2 percent by weight as determined by gas chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04276426 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-a9893f0bfb7241fdab297ba0c4e34031 |
| Source note | uspto-grants-1981_06 |